* 分析測試新成果

氯化鉀及聚乙二醇對聚脯氨酸-精氨酸液-液相分離的協(xié)同影響 ························································································································ 項東鑫，鄭 寓，周詩航，陸 奕，王艷偉 （ 1 ）

交流電弧原子發(fā)射光譜固體粉末樣品制備方法的改進 ·················· 郭心瑋，郝志紅，姚建貞，白金峰 （ 7 ）

分散固相萃取-超高效液相色譜-串聯(lián)質(zhì)譜法測定海龍中11 種磺胺類抗菌藥物殘留 ································································ 王小喬，李 堅，許曉輝，李劍勇，吳福祥，張虹艷，潘秀麗，李 赟 （ 16 ）

濾過型萃取柱-超高效液相色譜-串聯(lián)質(zhì)譜法同時測定水果中11 種農(nóng)藥殘留 ··················································································· 王子劍，趙勁松，郭曉宇，李 倩，鄭天馳，商愛媛，范 賽 （ 23 ）

藏藥訶子質(zhì)量標志物訶黎勒酸的標準化分析研究 ······························································································· 宋志博，陳 濤，王肖波，王岱杰，申 誠，王 碩，李洪梅，海 平，李玉林 （140）

敦煌莫高窟壁畫地仗層可溶鹽遷移過程模擬研究 ························ 錢 玲，呂功煊，胡紅巖，陳港泉 （149）

場發(fā)射掃描電子顯微鏡觀測弱導電金屬有機框架材料的參數(shù)探究 ······························································································································· 邢宏娜，常 帥，馮 偉，李興華 （160）

一價/二價陽離子濃度對蛋白質(zhì)-核酸液液相分離的調(diào)控 ················ 劉柱梁，鄭 寓，周詩航，王艷偉 （170）

堿性嫩黃O 的光電脫色工藝研究 ····························································································································· 倪賽迪，林秋涵，何碧珊，陳曉達，郭妙柃，栗鵬輝，林佳麗，陳毅挺 （178）

離子色譜法同時測定硫酸氫氯吡格雷中甲酸殘留及硫酸鹽含量 ·································································································································· 馮順卿，卓文珊，王瀟洋，劉洪濤 （185）

直鏈淀粉三(3, 5-二甲基苯基氨基甲酸酯)-聚醚砜手性膜色譜研究 ···················································································································· 普 娜，賴亞琳，高順秋，蔣雪菲，袁黎明 （280）

蒙藥十八味歐曲丸中游離汞的含量測定 ···································· 馬 蕊，丁玉竹，哈 偉，師彥平 （286）

基于鎳鉬硫化物納米花修飾碳納米管的腦利鈉肽電化學免疫傳感器的構(gòu)建 ··················································································································· 李 燕，朱長慧，代玉雪，李志英 （292）

頂空氣相色譜-電子捕獲檢測器法測定明膠空心膠囊中2-氯乙醇殘留量 ························································································································ 程 磊，郭文旭，王丹丹，陳 超 （299）

超聲萃取-氣相色譜法測定擬南芥種子中脂肪酸含量 ···················· 宜原原，羅 云，阮梅林，雷 敏 （339）

材料孔隙率測試方法的研究 ···················· 陳佩麗，宋 達，鄧金林，范明旸，陳曉麗，付 娟，蘇秋成 （347）

基于X射線光電子能譜的絕緣柵雙極型晶體管失效分析 ································································································································ 章小余，趙志娟，劉 芬，徐 鵬，屈寶龍 （352）

星狀風毛菊藥材分析及質(zhì)量標準研究 ·············································································································· 馬家麟，王 碩，陳 濤，宋 霞，喬亞玲，杲秀珍，申 誠，海 平，李玉林 （357）

* 大型儀器功能開發(fā)

正負壓一體式無空氣X射線光電子能譜原位轉(zhuǎn)移倉的開發(fā)及研制 ······························································································································· 章小余，趙志娟，袁 震，劉 芬 （ 30 ）

模擬空間原子氧輻照下X射線光電子能譜儀的原位表征功能開發(fā) ······························································································································· 劉 建，剡 珍，郝俊英，劉維民 （ 37 ）

高低溫環(huán)境下紅外光譜原位表征系統(tǒng)的研制 ···················· 郭 艷，許傳芝，王 嘉，張樂芬，牛建中 （ 43 ）

一種液體吸附原位紅外表征系統(tǒng) ··································· 郭 艷，許傳芝，王 嘉，張樂芬，牛建中 （216）

近紅外輕質(zhì)油品快速檢測系統(tǒng)的研制和應(yīng)用 ······························································ 陳國鈺 （221）

X-射線單晶衍射儀XtaLAB Pro 的低溫系統(tǒng)改造 ···································· 馬 宣，孫愛君，張 云 （227）

自補償型雙擺式干涉儀的設(shè)計 ················································ 石 磊，孫長庫，夏恒新，李巖松 （304）

* 大型儀器科學管理

高校儀器共享平臺檔案信息化管理模式探索 ······························ 李艷偉，盛弘強，方三華，劉 麗 （ 49 ）

我國民營第三方檢測服務(wù)現(xiàn)狀及趨勢 ···························································· 張志強，王麗紅 （334）

校級分析測試中心大型儀器設(shè)備共享平臺建設(shè)探討——以西南交通大學分析測試中心為例 ·················································································································· 衛(wèi)飛飛，方維臻 （429）

“四個最大”和“四個最小”的大型精密貴重儀器全生命周期管理體系的構(gòu)建 ················· 薛青松 （438）

* 浙江省大型科研儀器開放共享平臺—質(zhì)譜專欄

牛奶中全氟烷基酸的簡便萃取與定量研究 ············································ 李城華，汪 嫣，蔣可志 （ 54 ）

基于串聯(lián)質(zhì)量標簽定量質(zhì)譜法的膠質(zhì)瘤外泌體蛋白組差異分析 ··························· 裴順琪，譚 舟 （ 63 ）

基于氣相色譜三重四極桿質(zhì)譜法分析5 種苯系物在貽貝體內(nèi)的分布、蓄積和消除規(guī)律 ················································································ 晁鐸源，宋立玲，王紅光，丁 顒，邵宏宏，周秀錦 （ 68 ）

Cocktail 探針藥物法評價玄參對大鼠細胞色素P450 酶的影響 ····································································································· 魏艷麗，應(yīng)曉倩，談文狀，吳美玲，江悅娟，丁明星，杜洪建 （ 76 ）

質(zhì)譜在金屬有機框架材料結(jié)構(gòu)與應(yīng)用表征上的研究進展 ·························· 陳銀娟，丁傳凡，盧星宇 （ 83 ）

質(zhì)譜分析在變壓器所用礦物絕緣油成分分析中的應(yīng)用 ·················································· 劉佳蓉 （ 93 ）

離子色譜法測定廢水中的六氟磷酸根 ······································································· 趙 薇 （101）

* 分析測試經(jīng)驗介紹

加速溶劑萃取-QuEChERS-氣相色譜質(zhì)譜聯(lián)用法測定土壤中增塑劑 ······················· 唐會智，宋冬梅 （105）

原位變溫X射線衍射測試技術(shù)及其影響因素 ········· 毛 晶，郭倩穎，馬利利，龍麗霞，韓雅靜，馬曉暉 （111）

會理地區(qū)種植基地果蔬中農(nóng)藥殘留現(xiàn)狀與分析 ··································· 陳明華，曾 艷，歐陽衛(wèi)民 （117）

綜合物性測量系統(tǒng)振動樣品磁強計測量定中心問題的探究 ······················· 馬 麟，王 朔，王 維 （191）

利用Visual Basic 自動編制分析測試報告 ·································· 傅澤華，王如海，孫玉芳，唐昊冶 （197）

激光共聚焦顯微鏡測量表面粗糙度的探究 ············································ 廖奕鷗，馮 輝，張重遠 （203）

不同參數(shù)優(yōu)化對ZSM-5 分子篩的掃描電子顯微鏡圖像影響 ································ 王馨楠，高占明 （209）

木質(zhì)纖維素材料前處理的方法 ····································································· 王小曼，王 聞 （309）

無窗X射線能譜在熒光樣品與金屬鋰成分分析中的優(yōu)勢與經(jīng)驗摸索 ·················································································· 萬 鵬，蔡 蕊，李 勇，孟祥玉，周雨萌，高曉霞，徐 強，閆 肅 （313）

測量系統(tǒng)分析在大米鎘、鉛元素檢測中的應(yīng)用研究 ······················ 韋 冰，蔣菊媛，覃均生，張倩勉 （321）

電感耦合等離子體質(zhì)譜法測定鎂合金中的痕量元素 ····················································· 黃丹宇 （328）

QuEChERS-高效液相色譜/三重四極桿質(zhì)譜聯(lián)用法測定化妝品中防曬劑的檢測方法 ···················································································· 潘秀麗，邵長春，李 赟，許曉輝，王小喬，張虹艷 （384）

熟地黃的炮制及有效成分和微量元素的檢測研究 ···················································································································· 陳勝強，楊克培，康文利，周永昌，陶思曼，關(guān)伊辰，蒲秀瑛 （392）

粉末樣品制備方法對掃描電子顯微鏡成像質(zhì)量的影響 ·················································· 王馨楠 （400）

微波灰化-電感耦合等離子體發(fā)射光譜法測定嬰幼兒乳粉中的鈣和磷 ······································································································ 陳麗梅，張 慧，白國濤，馬彩霞，姚思雨，王 婧 （407）

苯系物相對質(zhì)量校正因子的測定與比較分析 ··················································· 李紫騰，李 盼 （414）

高效液相色譜法測定化妝品中類視黃醇含量 ······························ 羊潔芳，樓美娟，盧 力，姜士磊 （421）

* 綜 述

基于金屬有機框架材料的酶固定化策略及藥物篩選研究進展 ··························································································· 常香蕾，張 瑛，Stanislas Nsanzamahoro，王鋮博，王偉峰，楊軍麗 （125）

行波離子遷移譜技術(shù)及應(yīng)用研究進展 ························································································································· 潘慢慢，李 杭，徐一仟，楊其穆，蔣丹丹，王衛(wèi)國，陳 創(chuàng)，李海洋 （231）

原位高分辨微區(qū)元素分布特征檢測技術(shù)的應(yīng)用進展 ····················· 林梵宇，尹希杰，劉建鑫，孫延鑫 （245）

便攜式毒品傳感器的應(yīng)用與研究進展 ······································································· 楊 春 （261）

紫外光化學蒸氣發(fā)生技術(shù)綜述 ··························· 郭 煒，劉美彤，張衛(wèi)宏，葛迎吉，康 寧，劉子杰 （272）

地下建筑內(nèi)氡分布與去除技術(shù)研究進展 ··············································· 呂功煊，甄文龍，寧曉峰 （364）

* 大型儀器維護與維修

EA3000-CHNS 測試的影響因素與解決方案 ······························· 郭 毅，張瀅瀅，張歆寧，倪旭峰 （378）